Nanoscale synthesis and optical features of metallic nickel nanoparticles by wet chemical approaches
Identifieur interne : 000353 ( Main/Exploration ); précédent : 000352; suivant : 000354Nanoscale synthesis and optical features of metallic nickel nanoparticles by wet chemical approaches
Auteurs : Khalid Nouneh [Maroc] ; Munetaka Oyama [Japon] ; Raquel Diaz [Espagne] ; Mohammed Abd-Lefdil [Maroc] ; I. V. Kityk [Pologne] ; Mosto Bousmina [Maroc]Source :
- Journal of alloys and compounds [ 0925-8388 ] ; 2011.
Descripteurs français
- Pascal (Inist)
- Echelle nanométrique, Nickel, Nanomatériau, Sodium, Ethane-«1,2»-diol, Solution aqueuse, Réseau cubique, Dispersion, Synthèse nanomatériau, Spectre absorption, Absorption optique, Traitement surface, Oxyde d'indium, Oxyde d'étain, Nanostructure, Nanoparticule, Substrat oxyde d'indium et de zinc, Substrat InSnO, NaBH4, Polyol, 8116B, 7867B, 8107W.
- Wicri :
English descriptors
- KwdEn :
Abstract
Nickel nanoparticles (Ni-NPs) were successfully synthesized and attached on indium tin oxide (ITO) substrate by two different methods: from solution reduction process by using sodium borohydride (NaBH4) as reducing agent in the presence of poly(N-vinilpyrrolidone) (PVP) as protective and stabilizing agents and by polyol process under ethylene glycol EG as a solvent. The results indicated that the samples prepared in aqueous solution show the occurrence of face-centered cubic metallic nickel nanoparticles with a medium diameter of ∼31 nm and good size dispersion compared to the preparation in EG that revealed large size ∼150 nm. The dynamics of the nanoparticle's growth in the solvents and comparison with optical absorption is presented.
Affiliations:
- Espagne, Japon, Maroc, Pologne
- Communauté de Madrid, Rabat-Salé-Kénitra, Région du Kansai
- Kyoto, Madrid, Rabat
- Université autonome de Madrid, Université de Kyoto
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Le document en format XML
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<profileDesc><textClass><keywords scheme="KwdEn" xml:lang="en"><term>Absorption spectra</term>
<term>Aqueous solutions</term>
<term>Cubic lattices</term>
<term>Dispersions</term>
<term>Ethylene glycol</term>
<term>Indium oxide</term>
<term>Nanomaterial synthesis</term>
<term>Nanometer scale</term>
<term>Nanoparticles</term>
<term>Nanostructured materials</term>
<term>Nanostructures</term>
<term>Nickel</term>
<term>Optical absorption</term>
<term>Sodium</term>
<term>Surface treatments</term>
<term>Tin oxide</term>
</keywords>
<keywords scheme="Pascal" xml:lang="fr"><term>Echelle nanométrique</term>
<term>Nickel</term>
<term>Nanomatériau</term>
<term>Sodium</term>
<term>Ethane-«1,2»-diol</term>
<term>Solution aqueuse</term>
<term>Réseau cubique</term>
<term>Dispersion</term>
<term>Synthèse nanomatériau</term>
<term>Spectre absorption</term>
<term>Absorption optique</term>
<term>Traitement surface</term>
<term>Oxyde d'indium</term>
<term>Oxyde d'étain</term>
<term>Nanostructure</term>
<term>Nanoparticule</term>
<term>Substrat oxyde d'indium et de zinc</term>
<term>Substrat InSnO</term>
<term>NaBH4</term>
<term>Polyol</term>
<term>8116B</term>
<term>7867B</term>
<term>8107W</term>
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<term>Sodium</term>
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<front><div type="abstract" xml:lang="en">Nickel nanoparticles (Ni-NPs) were successfully synthesized and attached on indium tin oxide (ITO) substrate by two different methods: from solution reduction process by using sodium borohydride (NaBH<sub>4</sub>
) as reducing agent in the presence of poly(N-vinilpyrrolidone) (PVP) as protective and stabilizing agents and by polyol process under ethylene glycol EG as a solvent. The results indicated that the samples prepared in aqueous solution show the occurrence of face-centered cubic metallic nickel nanoparticles with a medium diameter of ∼31 nm and good size dispersion compared to the preparation in EG that revealed large size ∼150 nm. The dynamics of the nanoparticle's growth in the solvents and comparison with optical absorption is presented.</div>
</front>
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<country name="Japon"><region name="Région du Kansai"><name sortKey="Oyama, Munetaka" sort="Oyama, Munetaka" uniqKey="Oyama M" first="Munetaka" last="Oyama">Munetaka Oyama</name>
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